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Unveiling fine structure and energy-driven transition of photoelectron Kikuchi diffraction

Trung-Phuc Vo1,2, Olena Tkach3,4, Aki Pulkkinen1, Didier Sébilleau5, Aimo Winkelmann6, Olena Fedchenko7, Yaryna Lytvynenko3,8, Dmitry Vasilyev3, Hans-Joachim Elmers3 et al.

Gerd Schönhense3 and Ján Minár1,*

  • *Contact author: jminar@ntc.zcu.cz
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Phys. Rev. Research 8, 013151 – Published 10 February, 2026

DOI: https://doi.org/10.1103/wxcx-zt62

Abstract

The intricate fine structure of Kikuchi diffraction plays a vital role in probing phase transformations and strain distributions in functional materials, particularly in electron microscopy. Beyond these applications, it also proves essential in photoemission spectroscopy (PES) at high photon energies, aiding in the disentanglement of complex angle-resolved PES data and enabling emitter-site-specific studies. However, the detection and analysis of these rich faint structures in photoelectron diffraction, especially in the hard x-ray regime, remain highly challenging, with only a limited number of simulations successfully reproducing these patterns. The strong energy dependence of Kikuchi patterns further complicates their interpretation, necessitating advanced theoretical approaches. To enhance structural analysis, we present a comprehensive theoretical study of fine diffraction patterns and their evolution with energy by simulating core-level emissions from Ge(100) and Si(100). Using multiple-scattering theory and the fully relativistic one-step photoemission model, we simulate faint pattern networks for various core levels across different kinetic energies (106–4174 eV), avoiding cluster size convergence issues inherent in cluster-based methods. Broadening in patterns is discussed via the inelastic scattering treatment. For the first time, circular dichroism has been observed and successfully reproduced in the angular distribution of Si(100) 1s, revealing detailed features and asymmetries up to 31%. Notably, we successfully replicate experimental bulk and more “surface-sensitivity” diffraction features, further validating the robustness of our simulations. The results show remarkable agreement with the experimental data obtained using circularly polarized radiations, demonstrating the potential of this methodology for advancing high-energy PES investigations.

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Phys. Rev. Research 8, 013151– Published 10 February, 2026
  • Received 22 April 2025
  • Accepted 12 January 2026
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