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    Direct orientation contrast imaging of antiphase domains on III-V materials using scanning electron microscopy

    Brieg Le Corre1,2, Clothilde Grenèche1, Rozenn Bernard1, Tony Rohel1, Antoine Létoublon1, Wijden Khelifi1, Julie Le Pouliquen1, Arnaud Grisard3, Sylvain Combrié3 et al.

    Bruno Gérard4, Abdelmounaim Harouri2, Luc Le Gratiet2, Grégoire Beaudoin2, Konstantinos Pantzas2, Isabelle Sagnes2, Oliver Skibitzki5, Gilles Patriarche2, Charles Cornet1, and Yoan Léger1,*

    • *Contact author: yoan.leger@insa-rennes.fr

    Phys. Rev. Materials 10, 073804 – Published 20 July, 2026

    DOI: https://doi.org/10.1103/vl71-8m3d

    Abstract

    Direct orientation contrast imaging of zinc-blende III-V materials is studied using scanning electron microscopy. A quantitative approach is taken using a 3 µm thick orientation-patterned GaP grown on a GaAs sample, studying the antiphase domain contrast with respect to the electron beam energy and the tilt angle. A qualitative approach is taken for III-V grown on nonpolar materials with and without chemical mechanical polishing. Finally, a processing of the acquired image for GaP on Si reveals in-plane preferential antiphase boundaries.

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