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Complex spin structure and magnetic phase transition of Mn3−xFexSn alloys

W. Hanggai1,*, O. Hamutu1, G. A. de Wijs2, I. Dugulan1, N. H. van Dijk1, and E. Brück1

  • 1Fundamental Aspects of Materials and Energy (FAME), Faculty of Applied Sciences, Delft University of Technology, Mekelweg 15, 2629JB Delft, The Netherlands
  • 2Radboud University, Institute for Molecules and Materials, Heyendaalseweg 135, 6525AJ Nijmegen, The Netherlands

  • *Contact author: H.Gai@tudelft.nl
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Phys. Rev. B 112, 014407 – Published 7 July, 2025

DOI: https://doi.org/10.1103/pvjm-jvsr

Abstract

The hexagonal Mn3−xFexSn compounds possess several desirable properties that make them suitable magnetocaloric materials, including a ferromagnetic (FM)-to-paramagnetic (PM) transition near room temperature and soft magnetic behavior. In this study, we use the melt-spinning technique to explore the Mn-Fe-Sn ternary system. By combining magnetization measurements, Mössbauer spectroscopy, neutron diffraction (ND), oriented powder x-ray diffraction, and density functional theory (DFT) calculation, the magnetocaloric effect, spin structures, and the intrinsic magnetic properties of polycrystalline Mn3−xFexSn (x=0.8−1.4) compounds are determined. The FM-to-PM transition temperature TC ranges from 253 K (x=0.8) to 394 K (x=1.4). At low temperature, a spin reorientation at TS is observed, where below TS a coexistence of FM order with spins along the c axis and antiferromagnetic order with spins within the a−b plane occurs for x=0.8 and 1.0. However, for compounds with x=1.2 and 1.4, only FM order with spins along the c axis has been found below TS. Above TS, the spin structure corresponds to FM order with spins aligned within the a−b plane for all compositions. The magnetic moments of Mn and Fe were evaluated using DFT, demonstrating good agreement with the ND results.

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Phys. Rev. B 112, 014407– Published 7 July, 2025
  • Received 20 September 2024
  • Revised 6 February 2025
  • Accepted 21 May 2025
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