In quantum networks, after passing through noisy channels or information processing, residual states may lack sufficient entanglement for further tasks, yet they may retain hidden quantum resources that can be recycled. Efficiently recycling these states to extract entanglement resources, such as genuine multipartite entanglement or Einstein-Podolsky-Rosen pairs, is essential for optimizing network performance. Here, we develop a tripartite entanglement distillation scheme using an eight-photon quantum platform, demonstrating entanglement superactivation phenomena which are unique to multipartite systems. We successfully generate a three-photon genuinely entangled state from two biseparable states via local operations and classical communication, demonstrating superactivation of genuine multipartite entanglement. Furthermore, we extend our scheme to generate a three-photon state capable of extracting an Einstein-Podolsky-Rosen pair from two initial states lacking this capability, revealing a previously unobserved entanglement superactivation phenomenon. Our methods and findings offer not only practical applications for quantum networks, but also lead to a deeper understanding of multipartite entanglement structures.

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• Quantum channels
• Quantum communication
• Quantum communication, protocols & technology
• Quantum information theory
• Quantum networks